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Posted (edited)
warthog... Don't light too much of that stuff on the ground. Inhaling vaporized lead is a great way to get a lot into your body easily.

I don't light any of it on the ground. They all go skyward. wink2.gif

 

I don't take chances either, I wear my gloves and a mask when making them. I am dumb enough, don't need any help from lead. 2happy.gif

 

I would join in on the experimentation but right now I am not able to access the work site so no pyro for me for a bit.

Edited by warthog
Posted

 

If trying lead I would try first just keeping the ratios the same... Mix up a 10-20 gram batch and test. I have a high accuracy scale. It's necessary for making small amounts of comp when tuning. Tell me your results and we will go from there. I wouldn't recommend subcarbonate. The trioxides are where it's at! B)

 

 

Just tried my 1st batch w/lead. It burned very quicky, with minimal crackling (No Bang). It went straight to burn(Very bright).

 

One possible problem... The MgAl I used is 100 mesh, I used the formula for the 2.5-5mm eggs. As the formula specifies 100-200 mesh, I think this may be the problem.

 

I have 200-325 mesh MgAl, so I will try the smaller eggs with the base formula, and post my results.

 

If you have any suguestions I'd love to hear them.

Posted (edited)

Second Test using 200 - 325 MgAl (2mm eggs). It gave nearly the same results.

On a side note... I burned off the remainder of the first test batch, it burned like the individual eggs except at the very end I got one moderate pop. This leads me to beleave there is hope, but tweeking for the Bismuth formula will be required. I've got enough lead for another few tests, but wont be able to get to it for a few days. by then my Bismuth should be here.

 

 

 

I'll post any updates to my lead tests, and would welcome any input.

Edited by justhininabouti
Posted

where can a person even get Bismuth Trioxide these days? All my sources are out and say they will be for some time now.

 

I have NINE POUNDS of Red Lead though.... well, when it warms up I suppose I will se if I can get crackling. semi-pun intended. :)

Posted

where can a person even get Bismuth Trioxide these days? All my sources are out and say they will be for some time now.

 

I have NINE POUNDS of Red Lead though.... well, when it warms up I suppose I will se if I can get crackling. semi-pun intended. :)

 

 

USAPyro pointed me at uspigment.com. Note they call it Bismuth Oxide.

Posted
dang! They even have Realgar! Thanks!
Posted

Now if I could find some Bismuth Trioxide I could afford, I'd be in business. cool2.gif

 

That's the problem right there. $35 a pound. Ouch!

I'll probably just get some red lead.

Posted

I got my bismuth yesterday and ran a test batch using 200-325 MgAl. It gave the exact same results as my 2 batches using Lead (one with 200-325 and one with 100 MgAl), straigh to burn with small crackeling. As a test, I used USAPyro's Small egg formula (Optimized for 200-325 MgAl) using 100 MgAl, and it worked perfectly. My MgAl must be of a different grade then USAPyros.

 

I really like the reaction with the Bismuth, and I think that will make a great ent to a willow star of somethin similar. I'm going to put together a bigger batch, and try to put together some matrix stars.

 

 

 

Warthog - If you would like to collaborate on some Lead tests, it would sure be nice to get this effect from the cheaper lead, than having to use the costly bismuth. Let me know what you think.

Posted
justthininabouti, out of curiosity are you actually binding these mixtures into granules or burning them as powders? It isn't entirely clear.
Posted

justthininabouti, out of curiosity are you actually binding these mixtures into granules or burning them as powders? It isn't entirely clear.

 

 

Sorry about that. I have been binding them with alcohol as the solvent.

Posted (edited)
Justin, I would but right now the weather is all over the place here. One day it is nice and sunny and 60°F outside and the next day it is snowing or worse, freezing rain like it is now. Until Spring I am not really up for doing much at all except reading and now and then some work on my lance colors and burn rates. I am more than game to join in the experimentation when the season changes though. ;) Edited by warthog
Posted

Justin, I would but right now the weather is all over the place here. One day it is nice and sunny and 60°F outside and the next day it is snowing or worse, freezing rain like it is now. Until Spring I am not really up for doing much at all except reading and now and then some work on my lance colors and burn rates. I am more than game to join in the experimentation when the season changes though. ;)

 

I sure understand the weather thing. It's been similar here too. I'm working on some comets right now, But I'll get back to to the DE in a few days. Once I get some results, I'll start an new thread.

Posted (edited)

If they burn without cracking lower the oxidizer and MgAl amount. If they fail to smoulder go back one step. Lower the MgAl amount and don't change the oxidizer.

 

Sounds like your MgAl is more reactive than mine for some reason... So just lower the amount you use by 1/3rd and test again... Then if it works... Fine tune! If you have a working formula for a certain mesh MgAl post it. Bismuth dragon eggs are easy to fine tune once you get a feel for it. The issue is that different batches of MgAl can have different amounts of Al vs Mg, and mesh sizes may be more to a higher or lower range than labeled... Some may contain more reactive dust, and some may have been milled differently changing the reactivity. Etc... The only way to get perfect consistency is to alloy and grind the Mg and Al yourself.

 

The ratio of CuO to Bismuth Trioxide is unimportant in my experience. My dragon eggs work all the way from 15% bismuth to 50% and probably higher. (Only tested to there.) Best sound is with a decent amount of bismuth though. You can lower and raise the amount of bismuth and change the CuO accordingly and the composition still performs the same within a HUGE range.

 

Just follow these two rules and your good for tuning...

1. If it burns use less MgAl.

2. If it doesn't stay lit with a torch ignition use more MgAl.

 

If both of those rules fail... Change the amount of KClO4 and test over. I highly doubt those rules will fail you with bismuth and my main formula. When you shift the MgAl ratio up and down change CuO accordingly.

 

The KCLO4 oxidizer assists smoulder. It will prevent the crackling of dragon eggs in amounts over 7g and lead them straight to burn in my experience. Keep it in the 2-6g range. 3% is a good level to keep it at through the testing stage. It will assist smoulder and not cause any issues at that amount.

Edited by usapyro
  • 4 months later...
Posted

I've been mixing up different DE formulas for a while now. I can't seem to get it right.

I'm at work now so I don't remember the comp I used off hand- but I have to really heat'em up before they glow, and maybe pop-

when they do pop, it's a beautiful thing, really loud. I've tried rolling them as a star core but only maybe 5% of the eggs will pop as a star.

I also packed them in a fountain, but only got maybe 3 or 4 to pop. Tricky little buggers for sure!

 

They are about the size of a mouse turd- maybe I need to make them larger... I'll post the comp later when I get home this afternoon.

 

can't wait to get home- my order of star molecule is arriving today :D

Posted (edited)

the comp I'm using is:

 

bismith subcarbonate 75g

magnalium 200 mesh 15g

copper II oxide 10g

n.laquer 10%

 

the eggs are maybe 2-4 mm in size.

 

very hard to light even with a primer.

 

real loud pop when they do light.

Edited by NAC
Posted

I've been trying for some time to get my lead tetroxide eggs to work. I'm using the formula:

 

Lead Tetroxide 89%

MgAl (30-60 mesh) 11%

NC Lacquer 10%

 

will potassium perchlorate help at all? I know the dragon egg prime has potassium perchlorate in it... anyone have any other red lead formula?

  • 2 weeks later...
Posted (edited)

the comp I'm using is:

 

bismith subcarbonate 75g

magnalium 200 mesh 15g

copper II oxide 10g

n.laquer 10%

 

the eggs are maybe 2-4 mm in size.

 

very hard to light even with a primer.

 

real loud pop when they do light.

 

Try upping the CuO and lowering the bismuth. I had good success on my second batch ever using 37.5 CuO, 37.5 Bi2O3 25 MgAl (200 mesh) +10% NC

Reports say subcarbonate and trioxide are interchangeable 1:1.

 

I've been trying for some time to get my lead tetroxide eggs to work. I'm using the formula:

 

Lead Tetroxide 89%

MgAl (30-60 mesh) 11%

NC Lacquer 10%

 

will potassium perchlorate help at all? I know the dragon egg prime has potassium perchlorate in it... anyone have any other red lead formula?

 

I haven't used lead in dragon eggs so I may be mistaken - but shouldn't there be some CuO in your formula?

Edited by GalFisk
Posted
Yes there should be CuO, so that lead formula is never going to work.
Posted
You guys must have gotten some bad information along the way. I assure you that an all lead oxide comprised dragon eggs do indeed work. I can't say that I've ever seen an all bismuth oxide egg attempted, but that may just be a cost issue.
Posted

With only lead and MgAl?

 

I think it depends on how you define 'do indeed work', if it's small popping of the MgAl you want, then your right, if you mean an explosion, then you won't get that from that comp. Only sizzling stars.

  • 2 weeks later...
Posted

I got this off of pyroguide and have used the bismuth formula with great results. If you go to the site be sure your anti-virus is up to date, AVG is reporting the black hole trojan there. BTW, I have used a variation of magnalium size and have had good results with all

 

Lead-Copper Dragons eggs Lead tetraoxide (Minium) 44 Cupric oxide 31 Magnalium (60-200 mesh) 17 Sulphur 4 Potassium nitrate 4 Lead compounds are poisonous. Make sure to protect yourself!

Bismuth trioxide Dragon eggsBismuth trioxide or Bismuth subcarbonate 75 Magnalium (-200 mesh) 15 Copper (II) oxide (black) 10 Aluminium (atomized, -200 mesh) +5 Nitrocellulose lacquer10%

  • 7 months later...
Posted
i have everything for this and i hate nc ..have to give this some sertous props
Posted
whatever happened to USApyro? Anybody know if he's alive and well?
  • 3 months later...
Posted
i just got my trioxide today. all i have is 200-325 mesh mag/al gonna make a test batch tomorrow..
Posted
i followed the comp for the 200-325 mesh mag/al worked perfectly my first batch.and i only used meal-d for the prime.after drying i just spray them with some denatured alchohol and rolled them in a couple of layers of meal-d. simplicity at its finest :D
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